The MWL120 Real-Time Back-Reflection Laue Camera System from Multiwire Laboratories
MWL120 System

At last — a Laue camera that rapidly orients and characterizes single crystals (in a matter of seconds!)


Highlights

  • Ideal replacement for the Polaroid XR-7 back-reflection cassette (film no longer available)
  • Northstar 7 software indexes Laue images from cubic, hexagonal, ...triclinic crystal systems and generates stereographic projections
  • Provides an accuracy of 0.25° in standard mode and 0.05° in high-resolution mode
  • Applications include: silicon, gallium arsenide, high-Tc superconductors, sapphire, geological minerals, turbine blades, etc. and detecting grain boundaries
  • Ideal for industrial process control, research applications, or academic laboratories
  • Earlier model MWL110 systems can be upgraded to 120 capability

What is the MWL120 System?

The back-reflection Laue method

The MWL120 allows an operator to orient single crystals quickly and easily. Manipulate the orientation of a crystal sample using our joystick-controlled motorized stages and see the diffraction pattern move in real time on a computer monitor to rapidly characterize or determine the orientation of the crystal's lattice planes.

The MWL120 system uses the back-reflection Laue method. The Laue camera interfaces with an X-ray tower and collimates the beam through the center of the camera toward the crystal sample. These X-rays then reflect off the sample back to the detector where the diffraction pattern is collected. This information is piped to a computer running NorthStar 7 — the latest version of our powerful orientation software — and is displayed in real time.


More on NorthStar 7

NorthStar doesn't just display real-time diffraction patterns. It can also collect images with increased exposure-time, find the Laue spots, and then index most of these images automatically once suitable imaging conditions are established. The 'Find Extra Planes' feature even shows the computed plane position oriented behind the collimator which you can't otherwise see when perfectly oriented!

NorthStar 7 is the culmination of years of development work and is a great improvement over other available Laue software, especially in the area of ease of use.

NorthStar 7 ...

  1. Accommodates small variations in the film-to-specimen distance
  2. Controls the percentage of Laue spots to be indexed (troublesome points can be ignored, if needed)
  3. Tries multiple combinations of starting Laue points and selects the best orientation matrix automatically
  4. Features "shortcut icons" for faster manual work and a "macro" facility for one-touch analysis of crystal orientation. Once set with the right conditions, novice users can achieve expert results quickly with very little effort.

How has the MWL120 improved from the older MWL110 system?


Examples

Collected and Real-Time Laue Images

Silicon 110 Axis Collected Laue Image in 256 Mode
Collected Laue Image of a Silicon Crystal in 110 Orientation
Gallium Arsenide real time image in arbitrary orientation
Gallium Arsenide Real-Time Image
in Arbitrary Orientation
Germanium 111 Axis in Real-Time 512 Mode
Germanium Real-Time Image Showing 3-fold Symmetry — or 111 Orientation


Stereographic Projection

Silicon 110
NorthStar has Autodetected 14 Laue Spots in this Silicon 110 Image
The autodetection thresholds can be adjusted to find fainter spots, but a selection of 14 points is more than enough to index this image
Silicon 110
The Points Have Been Indexed
In other words, Miller indices have been calculated for the selected Laue points from an orientation matrix. Because the 'Find Extra Planes' feature was enabled, NorthStar was able to generate information for the 110 plane at the center of the image. This plane is 0.6° offset from the center — 0.2° right and 0.5° up
Silicon 110 Stereographic Projection
A Stereographic Projection has been Generated
The hkℓ solution has been projected onto a plane, and the previously selected Laue spots are drawn in red on the projection. In NorthStar, clicking any point will rotate the orientation matrix and center the projection on that point
Stereo Plot Control
The Stero Plot Control
These tools allow the operator to manually rotate the orientation matrix behind the stereographic projection as an alternative to clicking a spot. Once the crystal sample has been virtually oriented using either method, the angles in the X, Y, and Z fields will inform the operator how to physically rotate the crystal sample. Click here for a more detailed example

Lead time for an MWL120 system can vary from 30 to 90 days. See here for pricing.

Multiwire Laboratories, Ltd.